Improvement of the Productivity of Preparation Process for Ultrafine Metal Sulfide Particles Using Reverse Micellar Systems
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概要
- 論文の詳細を見る
An improvement of the productivity of the preparation process for ultrafine ZnS and CdS particles using sodium bis(2-ethylhexyl) sulfosuccinate (AOT)/isooctane reverse micellar systems is studied. Sufficient quantities of reactants are provided to the reverse micelles by using H2S gas and the functionalyzed surfactants, Zn(AOT)2 and Cd(AOT)2. Bis(2-ethylhexyl) sulfosuccinic acid formed as by-product restrains the formation of ZnS particles, and destabilizes the CdS particles. Neutralization of the acid by addition of an alkaline reagent, triisooctylamine, improves the conversion for ZnS particles and the stability for CdS particles. Ultrafine ZnS and CdS particles containing about 0.02 M of constituting ions are successfully prepared in the presence of the amine. The particles can be recovered from the reverse micelles and redispersed in non-micellar solvent via the surface capping of the particles with thiols. The proposed route using reverse micelles is applicable for the practical production of ultrafine particles.
- 社団法人 化学工学会の論文
著者
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SATO Hiroshi
Department of Cardiovascular Medicine, Osaka University Graduate School of Medicine
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Komasawa Isao
Department of Chemical Science and Engineering, Graduate School of Engineering Science, Osaka Univer
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駒沢 勲
Department Of Chemical Science And Engineering Graduate School Of Engineering Science And Research C
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Komasawa Isao
Department Of Chemical Science And Engineering Graduate School Of Engineering Science Osaka Universi
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OHTSU Takeshi
Department of Chemical Science and Engineering, Graduate School of Engineering Science, Osaka Univer
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Ohtsu Takeshi
Department Of Chemical Science And Engineering Graduate School Of Engineering Science Osaka Universi
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Komasawa Isao
Department Of Chemical Engineering Faculty Of Engineering Science Osaka University
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佐藤 博
大阪大学 大学院基礎工学研究科
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Sato Hiroshi
Department Of Anatomy And Developmental Neurobiology Institute Of Health Biosciences The University
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