Preparation of Ultrafine Palladium Particles in Reverse Micelles and Application for Hydrogenation Catalysts
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概要
- 論文の詳細を見る
The preparation of ultrafine Pd and Pd-Au particles, in AOT (sodium bis(2-ethylhexyl) sulfosuccinate), CTAC (cetyltrimethylammonium chloride) and C18E7 (polyoxyethylene (7) oleyl ether) reverse micelles, using KBH4 as a reducing agent, has been studied. Excess KBH4 is required, because part of this is lost by hydrolysis and also by reduction of the surfactants. The particles in reverse micellar solution exhibit an activity for the hydrogenation of both water-soluble allyl alcohol and water-insoluble styrene, but the activity is inhibited by the surfactant molecules. Immobilization of the particles on solid supports, derivatized with a thiol-terminated silane, was carried out, aiming at possible applications as supported catalysts. The supported catalysts also exhibit hydrogenation activity, when the surfactant molecules are removed from the surface of the catalysts by calcination.
- 社団法人 化学工学会の論文
- 2002-03-01
著者
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SATO Hiroshi
Department of Cardiovascular Medicine, Osaka University Graduate School of Medicine
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Komasawa Isao
Department of Chemical Science and Engineering, Graduate School of Engineering Science, Osaka Univer
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駒沢 勲
Department Of Chemical Science And Engineering Graduate School Of Engineering Science And Research C
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Komasawa Isao
Department Of Chemical Science And Engineering Graduate School Of Engineering Science Osaka Universi
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OHTSU Takeshi
Department of Chemical Science and Engineering, Graduate School of Engineering Science, Osaka Univer
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Ohtsu Takeshi
Department Of Chemical Science And Engineering Graduate School Of Engineering Science Osaka Universi
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Komasawa Isao
Department Of Chemical Engineering Faculty Of Engineering Science Osaka University
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佐藤 博
大阪大学 大学院基礎工学研究科
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Sato Hiroshi
Department Of Anatomy And Developmental Neurobiology Institute Of Health Biosciences The University
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