脂肪酸分析のための蛍光誘導体化試薬9-アントラセンメタノールの精製
スポンサーリンク
概要
- 論文の詳細を見る
A fluorescent-labeling reagent 9-anthracenemethanol was purified by recrystallization for use in microanalysis of natural oil fatty acids. A commercial reagent was dissolved in ethyl acetate at the boiling point, and allowed to stand at room temperature until the crystals precipitated in yellow needles. The product given in the yield of 74% was analyzed by reversed-phase high-performance liquid chromatography. Many contaminant peaks found in the crude material disappeared in the chromatogram, indicating successful purification of the reagent. The purified reagent could be used for fatty acid analysis of 1-5μg of natural triacylglycerols including those of cod liver/mackerel oil and bonito head oil. 2-Butanone was also effective solvent for the purification. With these solvents, commercially available 9-anthracenemethanol can be purified by the simple recrystallization.
- 2009-12-08
著者
-
安藤 靖浩
北海道大学大学院水産科学研究院
-
安藤 靖浩
北大・水産
-
安藤 靖浩
北海道大学水産学部海洋生物資源化学科
-
Ando Yasuhiro
Department Of Marine Bioresources Chemistry Faculty Of Fisheries Hokkaido University
-
Ando Yasuhiro
Division Of Marine Life Sciences Faculty Of Fisheries Science Hokkaido University
-
ANDO Yasuhiro
Graduate School of Fisheries Sciences, Hokkaido University
-
Ando Yasuhiro
Department of Marine Bioresources Chemistry, Faculty of Fisheries, Hokkaido University,
関連論文
- ツノナシオキアミEuphausia pacificaの密度比,音速比の変化とターゲットストレングス推定に与える影響
- Reversible acute renal failure associated with clomipramine-induced interstitial nephritis
- Renal Screening Tests
- Reduced peritoneal protein selectivity may indicate peritoneal fibrosis in CAPD patients
- DHA高含有魚油TGにおける脂肪酸の位置分布 : 食品
- ニンジン種子油のトリアシルグリセリンの立体構造
- Lipids and Fatty Acids in Artemia Nauplii Enriched with Fish Oil Triacylglycerols Containing Docosahexaenoic Acid in Different Positional Distribution Patterns
- Fatty Acid Enrichment of Rotifers Using Type-A Gelatin Solution
- Lipid Profile of Mysid Neomysis intermedia and Its Changes by Feeding DHA-Rich Marine Lipids
- 脂肪酸分析のための蛍光誘導体化試薬9-アントラセンメタノールの精製
- Deleterious effect of diatom diets on egg production and hatching success in the marine copepod Pseudocalanus newmani
- Reinvestigation of positional distribution of tetracosahexaenoic acid in triacyl-sn-glycerols of flathead flounder flesh
- トリアシルグリセロールの立体特異分析
- Identification of 5-Octadecenoic Acid in the Rotifer Brachionus plicatilis
- Rapid Preparation of Fluorescent 9-Anthrylmethyl Esters for Fatty Acid Analysis of Small Amount of Triacylglycerols
- Fatty acid composition of two species of Japanese freshwater sponges Heterorotula multidentata and Spongilla alba
- Positional Distribution of DHA in Triacyl-sn-glycerols of Artemia Nauplii Enriched with Salmon Roe Polar Lipids-Containing Fish Oil
- Distribution of Novel Nonmethylene-Interrupted Fatty Acids over Neutral and Polar Lipids of Ophiuroidea (Brittle Star)
- キラルカラム高速液体クロマトグラフィーを用いたトリアシルグリセリンの立体特異分析部分加水分解物の直接誘導体化
- キラルカラム高速液体クロマトグラフィーによるトリアシルグリセリンのアシル基分布の立体特異分析
- Tumoral calcinosis associated with hypercalcemia in a patient with chronic renal failure
- Phagostimulant Activity of Phosphatidylcholine Molecular Species for Young Abalone Haliotis discus hannai
- Demospongic Acids of the Marine Sponge Halichondria panicea from the Coast of Hokkaido, Japan
- HPLCによるトリアシルグリセロールの立体特異分析
- Occurrence of all-cis-5,8,11,14,17,20,23-hexacosaheptaenoic acid (26:7n-3) in roughscale sole Clidoderma asperrimum flesh lipids
- Gas Chromatographic Separation of Docosenoic Acid Positional Isomers on an SLB-IL100 Ionic Liquid Column
- Accelerated recovery from nephrotic syndrome with acute renal failure by double filtration plasmapheresis in a patient with lupus podocytopathy
- 脂肪酸分析のための蛍光誘導体化試薬 9-アントラセンメタノールの精製
- Acute Kidney Injury in a Patient with Nephrotic Syndrome due to Focal Segmental Glomerular Nephritis Induced by a Single Oral Administration of High-dose Bisphosphonate (Minodronate)
- A Case of Insulin-Resistant Diabetes Mellitus Successfully Treated with Plasmapheresis in a Chronic Hemodialyzed Patient(Diabetes Mellitus,General Presentation)
- Comparison between serum free triiodothyronine levels and body fluid distribution in hemodialysis patients