アルギン酸誘導体の製造及び利用に関する研究-IV : GORDON-SCHOTTEN-BAUMANN法によるアルギン酸のパルミトイル化について
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Various conditions were examined at the palmitoylation of alginic acid by the modified SCHOTTEN-BAUMANN process, with which GORDON et al. prepared the palmitoyl protein. In our experiments, good yield was obtained when 1) the concentration of alginic acid in aqueous solution was 1 %, 2) the weight of ether was 5 times as much as palmitoyl chloride, 3) the time of agitation was 20-30min. after the addition of reactant, etc.
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