2(E)-(4-Methyl-3-pentenylidene)-butanedial, β-Acaridial: A New Type of Monoterpene from the Mold Mite Tyrophagus putrescentiae(Acarina, Acaridae)(Organic Chemistry)

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• The natural product chemistry of opisthonetal gland excretion was studied for the mold mite Tyrophagus putrescentiae. The secretion contained a new type of mono-terpene dial, 2(E)-(4-methyl-3-pentenylidene)-butanedial (1), which we gave the trivial name β-acaridial. The compound was synthesized by a Wittig reaction of 4-methyl-3-pentenyltriphenylphosphonium bromide with 1,4-tetrahy-dropyranoxy-2-oxobutane (derived from the hydration of 2-butyn-1,4-diol with HgSO_4 and H_2SO_4, and subsequent protection of the hydroxy groups as tetrahydropyranoxy ether), deprotection of the hydroxy groups, and subsequent oxidation with PDC. The synthetic dialcohol was identical to β-acaridiol obtained by the reduction of the natural product.

• 社団法人日本農芸化学会の論文
• 1989-03-23

著者

• Leal W

  Institute Of Applied Biochemistry University Of Tsukuba:(present Office)national Institute Of Sericu

• Leal Walter

  National Institute Of Sericultural And Entomological Science

• Leal Walter

  Institute Of Applied Biochemistry University Of Tsukuba:(present Office)national Institute Of Sericu

• KUWAHARA Yasumasa

  Institute of Agriculture and Forestry, University of Tsukuba

• SUZUKI Takahisa

  Institute of Applied Biochemistry, University of Tsukuba

• Leal W

  Univ. California Davis Ca Usa

• Sakata T

  Pesticide Research Institute Faculty Of Agriculture Kyoto University

• Suzuki Takahisa

  Institute Of Applied Bichemistry University Of Tsukuba

• Kuwahara Yasumasa

  Institute Of Agriculture And Forestry University Of Tsukuba

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