Fluorometric Determination of Diarrhetic Shellfish Toxins by High-Performance Liquid Chromatography(Analytical Chemistry)
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概要
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Two principal toxins of diarrhetic shellfish poisoning, okadaic acid and diophysistoxin-1, were esterified with 9-anthryldiazomethane in methanol. After cleaning with a Sep-pak silica cartridge column, the fluorescent esters were analyzed on a Develosil ODS column with MeCN-MeOH-H_2O (8:1:1). The fluorescence intensities of both toxin derivatives measured at an excitation of 365 nm and an emission of 412 nm showed good linearity in the range 1〜80 ng.
- 社団法人日本農芸化学会の論文
- 1987-03-22
著者
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Lee Jong
Laboratory Of Applied Entomology Faculty Of Agriculture Yamaguchi University
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Lee Jong
Laboratory Of Food Hygiene Faculty Of Agriculture Tohoku University
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YASUMOTO Takeshi
Laboratory of Bio-organic Chemistry, Department of Applied Biological Chemistry, Faculty of Agricult
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Yanagi Toshihiko
Laboratory Of Food Hygiene Faculty Of Agriculture Tohoku University
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KENMA Ritsuko
Laboratory of Food Hygiene, Faculty of Agriculture, Tohoku University
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Yasumoto Takeshi
Laboratory Of Food Hygiene Faculty Of Agriculture Tohoku University
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Yasumoto Takeshi
Laboratory Of Bio-organic Chemistry Department Of Applied Biological Chemistry Faculty Of Agricultur
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Kenma Ritsuko
Laboratory Of Food Hygiene Faculty Of Agriculture Tohoku University
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