PREPARATION OF NICKEL ALUMINUM DOUBLE HYDROXIDES FROM HEXAAMMINENICKEL (II) COMPLEX SOLUTION
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概要
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Nickel aluminum double hydroxides, Ni_<1-x>Al_x (OH)_2 (CO_3)_<x/2>・mH_2O, were prepared from a hexaamminenickel (II) complex solution by the addition of mixed solutions of aluminum nitrate and sodium hydroxide. The crystallinity of the products was better than that of the double hydroxides prepared by a conventional coprecipitation method. Based on the relationship between the layer spacing and the atomic fraction Al/(Al+Ni) in the products [=R (pro)], the range for the formation of the single phase products was determined to be 0.19≤R (pro)≤0.33. In this range the layer spacing diminished with the increase in R (pro). IR and DTA results also indicated the variation in the layer charge caused by the aluminum substitution. The anion exchange capacity was 1.5-2.6 meq/g within the soild solution range. The thermal behavior of the products was also investigated.
- 日本粘土学会の論文
著者
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PARK In
Department of Dental Anesthesiology, Clinic for Persons with with Disabilities, Seoul National Unive
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Park I
Department Of Applied Chemistry Waseda University
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Park In
Department Of Materials Science And Engineering Hanbat National University
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KURODA KAZUYUKI
Department of Applied Chemistry, Waseda University
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KATO CHUZO
Department of Applied Chemistry, Waseda University
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Kuroda Kazuyuki
Department Of Applied Chemistry And Kagami Memorial Laboratory For Materials Science And Technology
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Kato C
Department Of Applied Chemistry Waseda University
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Kato Chuzo
Department Of Applied Chemistry School Of Science And Engineering Waseda University
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Kuroda K
Department Of Applied Chemistry School Of Science And Engineering Waseda University:kagami Memorial
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Park In
Department of Applied Chemistry, Waseda University
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