Synthesis of Peptides with α, β-Dehydroamino Acids. XIII Photoisomerization of Ac-(Z)-Δ-Phe-NHMe : Ac-(E)-ΔPHe-NHMe

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概要

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• Easily accessible Ac-(Z)-ΔPhe-NHMe was photoisomerized to so far unknown Ac-(E)-ΔPhe-NHMe. Some parameters of the process leading to a diastereomeric mixture of ratio 90(Z) : 10(E) have been tested and the photoisomerization has been carried out on a preparative milligram scale. The isomers were separated via crystallization followed by preparative HPLC.

• 公益社団法人日本薬学会の論文
• 2000-02-01

著者

• RZESZOTARSKA Barbara

  Department of Organic Chemistry, University of Opole

• Rzeszotarska Barbara

  Department Of Organic Chemistry University Of Opole

• KUBICA Zbigniew

  Department of Organic Chemistry, University of Opole

• KOZLECKI Tomasz

  Faculty of Chemistry, University of Wroclaw

• Kubica Zbigniew

  Department Of Organic Chemistry University Of Opole

• Kozlecki Tomasz

  Faculty Of Chemistry University Of Wroclaw

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• Synthesis of Peptides with α, β-Dehydroamino Acids. XIII Photoisomerization of Ac-(Z)-Δ-Phe-NHMe : Ac-(E)-ΔPHe-NHMe

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