A Large Scale Synthesis of Mono- and Di-urethane Derivatives of Lysine

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概要

• 論文の詳細を見る

• In the search for a practical route to lysine diurethane derivatives useful for peptide synthesis, we elaborated the synthesis of N^ε-tert-butoxycarbonyl-L-lysine copper(II) complex (1). This served as substrate for obtaining N^ε-tert-butoxycarbonyl-L-lysine (2), N^α-benzyloxycarbonyl-N^ε-tert-butoxycarbonyl-L-lysine dicyclohexylamine salt (3) and N^α-(9-fluorenyl)methoxycarbonyl-N^ε-tert-butoxycarbonyl-L-lysine (4).

• 公益社団法人日本薬学会の論文
• 1999-10-15

著者

• Rzeszotarska B

  Institute Of Chemistry University Of Opole

• WIEJAK Stanislaw

  Laboratory of Chemistry, Technical University of Opole

• MASIUKIEWICZ Elzbieta

  Department of Organic Chemistry, University of Opole

• RZESZOTARSKA Barbara

  Department of Organic Chemistry, University of Opole

• Rzeszotarska Barbara

  Department Of Organic Chemistry University Of Opole

• Wiejak Stanislaw

  Laboratory Of Chemistry Technical University Of Opole

• Masiukiewicz E

  Institute Of Chemisty University Of Opole

• Masiukiewicz Elzbieta

  Department Of Organic Chemistry University Of Opole

関連論文

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• Synthesis, Structure and Properties of N-Acetylated Derivatives of Methyl 5-Amino-1H-[1,2,4]triazole-3-carboxylate
• Improved Scalable Syntheses of Mono- and Bis-Urethane Derivatives of Ornithine
• The Molecular and Crystal Structure of tert-Butyl N^α-tert-Butoxycarbonyl-_L-(S-trityl)cysteinate and the Conformation-Stabilizing Function of Weak Intermolecular Bonding
• A Large Scale Synthesis of Mono- and Di-urethane Derivatives of Lysine
• Convenient High Yielding Gram Scale Solution Synthesis of Methionine-Enkephalin
• Synthesis of Peptides with α, β-Dehydroamino Acids. XIII Photoisomerization of Ac-(Z)-Δ-Phe-NHMe : Ac-(E)-ΔPHe-NHMe

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