Syntheses of Allied Compounds of Lupine Alkaloids. V. Synthesis of 9-Azahexahydrojulolidine

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概要

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• 9-Azahexahydrojulolidine (III) was prepared by saponification and decarboxylation of 2-cyanoperhydropyrido [3,4,5-i, j] quinolizine (II) with hydrochloric acid, obtained by reaction of 9-methyl-9-azahexahydrojulolidine (I) and cyanogen bromide. Series of these compounds was assumed to have the cis-quinolizidine ring and, in order to ascertain this assumption, (III) was converted to 9-azajulolidine (IV).

• 公益社団法人日本薬学会の論文
• 1959-10-20

著者

• 佐藤 義信

  Takamine Research Laboratory Sankyo Co. Ltd.

• 佐藤 義信

  Takamine Research Laboratory, Sankyo Co., Ltd.

関連論文

• Syntheses of 2-Hydroxymethylnicotinic Acid Lactone, 2-Hydroxymethylpyridine-3-acetic Acid Lactone, and Some of their Derivatives
• Syntheses of Allied Compounds of Lupine Alkaloids. V. Synthesis of 9-Azahexahydrojulolidine
• Synthesis of 5-Hydroxymethylquinoline-4-carboxylic Acid Lactone.
• Syntheses of Allied Compounds of Lupine Alkaloids. IV. Synthesis and Hydrogenation of 4-Oxo-4H-quinolizine Derivatives.
• Syntheses of Allied Compounds of Lupine Alkaloids. III. Synthesis of 3,6-Dioxo-1H, 3H, 6H-pyrano [3,4,5-i, j] quinolizine.
• Synthesis of 3-Oxo-10a, 1-dihydropyrano [3,4,5-i, j]-6-oxoquinolizine
• The Synthesis of Lupine Alkaloids. II. The Synthesis of 1-(α-Piperidyl) quinolizidine.
• Lupinアルカロイドの合成(第1報) : Sparteine新異性体の合成
• The Migration of Benzyl Group from Nitrogen to the Carbon in the Methyl Group of α-and γ-Picolines.

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