Synthesis of N, N-Dimethyl-2-(tributylstannyl)methyl-5-substituted Benzylamines as a Quinodimethane Precursor by the Reaction of N, N-Dimethyl-N-(tributylstannyl)methyl-4-substituted Benzylammonium Salts with Lithium Diisopropylamide
スポンサーリンク
概要
- 論文の詳細を見る
Reaction of N, N-dimethyl-N-(tributylstannyl)methyl-4-substituted benzylammonium salts 2 with lithium diisopropylamide (LDA) gave N, N-dimethyl-2-(tributylstannyl)methyl-5-substituted benzylamines 3 as the main products. Treatment of 3 with iodomethane followed by tetrabutylammonium fluoride (TBAF) in the presence of dimethyl fumarate gave the corresponding dimethyl trans-1,2,3,4-tetrahydro-6-substituted naphthalene-2,3-dicarboxylates 15 in good yields.
- 公益社団法人日本薬学会の論文
- 1998-03-15
著者
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Maeda Yasuhiro
Faculty Of Engineering Osaka Prefecture University
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Sato Yoshiro
Faculty Of Pharmaceutical Science Nagoya City University
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Maeda Yasuhiro
Faculty Of Pharmaceutical Science Nagoya City University
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- Synthesis of N, N-Dimethyl-2-(tributylstannyl)methyl-5-substituted Benzylamines as a Quinodimethane Precursor by the Reaction of N, N-Dimethyl-N-(tributylstannyl)methyl-4-substituted Benzylammonium Salts with Lithium Diisopropylamide