4-(7-Diethylaminocoumarin-3-yl)benzoyl Cyanide (DACB-CN) : A Highly Sensitive Fluorescent Derivatization Reagent for Alcohols in High-Performance Liquid Chromatography
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概要
- 論文の詳細を見る
4-(7-Diethylaminocoumarin-3-yl)benzoyl cyanide (DACB-CN) was synthesized as a new fluorescent derivatization reagent for alcohols for use in high-performance liquid chromatography. Saturated alcohols (C_8-C_<22>) were derivatized in good yields to give the corresponding fluorescent DACB-esters by treatment with DACB-CN. The DACB-esters of these alcohols were clearly separated on a reversed-phase HPLC column. The detection limit (S/N=3) of cetyl alcohol, a test compound, was 1-2 fmol/10 μl.
- 公益社団法人日本薬学会の論文
- 1998-01-15
著者
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Machida Minoru
Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido
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Goto Yasuo
Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido
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Takechi Haruko
Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido
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