A simple synthesis of (.+-.)-cis-(6-methyltetrahydro-2-pyranyl)acetic acid, a constituent of civet.

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概要

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• The title compound was synthesized stereoselectively starting with readily available 5-hexanolide in a 47% overall yield.

• 公益社団法人 日本化学会の論文

著者

• Suginome Hiroshi

  Organic Synthesis Division, Department of Chemical Process Engineering, Faculty of Engineering, Hokkaido University

• Kobayashi Kazuhiro

  Organic Synthesis Division, Department of Chemical Process Engineering, Faculty of Engineering, Hokkaido University

関連論文

• Replacement of a carbonyl group of camphor by an oxygen atom. Synthesis of 1,7,7-trimethyl-2-oxabicyclo(2.2.1)heptane.
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• Photo- and thermally-induced radical rearrangements of 6-methyl- and 4,4,6-trimethylcholest-5-en-3.BETA.-ol.
• A simple synthesis of (.+-.)-cis-(6-methyltetrahydro-2-pyranyl)acetic acid, a constituent of civet.
• Photoinduced molecular transformations. 114. An efficient synthesis of 5,7-dihydroxy-4-methylisobenzofuran-1(3H)-one, a metabolite of aspergillus flavus and a key intermediate in the synthesis of mycophenolic acid.

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