実験室における有機電極合成の実際

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This article contains a variety of laboratory-scale experimental methods for electroorganic synthesis, which may probably give practical guidelines or some clues to a synthetic organic chemist who has not been famililar with this specific but useful technique in organic synthesis in spite of his much interest. Following items are explained mainly in order to seek good answers for many problems, such as how to get easy availability of equipment, simplicity of procedure, solution of various experimetal trouble and optimum reaction conditions. 1) Preface 2) Equipment to prepare. 3) Various type of methods and practical examples of electroorganic synthesis. 4) Experimental factors controlling electroorganic reaction -Searching of optimum reaction conditions- 5) Final comment As this specific reaction may be generally controlled by more experimental factors than ordinary chemical reaction in solution, more “try and error” may be required to get optimum conditions, hopefully, by simpler equipment and procedure.
社団法人有機合成化学協会の論文