Synthesis and exfoliation of layered hydroxide zinc aminobenzoate compounds

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概要

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• Two types of layered hydroxide zinc o-aminobenzoate compounds with structures of layered basic metal salt (LBMS) were prepared by reacting of zinc hydroxide and o-aminobenzoic acid solution in a temperature range of 40-110°C. The formation reactions, structures, chemical compositions, and exfoliation behavior in alcohol solvents of the layered compounds were investigated by using XRD, TG-DTA, SEM, and TEM. The layered phase with a basal spacing of 1.33 nm has an a-Ni(OH)2-like structure, and its chemical formula can be written as Zn(OH)1.27(o-NH2C 6H4COO)0.73·nH2O. The 1.33 nm layered phase shows plate-like particle morphology. The plate-like crystals can be exfoliated into nanosheet-like particles in alcohol solvents.

著者

• Feng Qi

  Department Of Advanced Materials Science Faculty Of Engineering Kagawa University

• Ishikawa Yoshie

  Department of Advanced Materials Science, Faculty of Engineering, Kagawa University

• ZHAO Lifang

  Department of Chemistry and Chemical Engineering, Baoji University of Arts and Science

• MIAO Jianyjing

  Department of Chemistry and Chemical Engineering, Baoji University of Arts and Science

• WANG Hongshe

  Department of Chemistry and Chemical Engineering, Baoji University of Arts and Science

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