Analysis of the Toad Poison Bufadienolides by Rod-Thin-Layer Chromatography with Flame Ionization Detector

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概要

• 論文の詳細を見る

• "Analysis of the toad poison bufadienolides using the rod-thin-layer chromatography (Rod-TLC) with FID was undertaken. By the use of n-hexane/CH_2Cl_2/MeOH(11 : 8 : 1) as a developing solvent system, an effective separation of the eight bufadienolides-cinobufagin, resibufogenin, bufalin, bufotalin, desacetyl-cinobufagin, desacetyl-bufotalin, gamabufotalin and 3-oxo-cinobufagin-was obtained. Also, the reactivities of cinobufagin in oxidation and hydrolysis by using reaction mixture were checked by Rod-TLC. The contents of three major bufadienolides-resibufogenin, cinobufagin and bufalin-in the two kinds of Ch'an Su (the so-called ""disk-like Ch'an Su"" and ""thin-plate Ch'an Su"") were analyzed by the use of Rod-TLC (IATROSCAN)."

• 神奈川大学の論文

著者

• Pettit G

  Cancer Research Institute And Department Of Chemistry Arizona State University

• Pettit George

  Cancer Research Institute And Department Of Chemistry Arizona State University

• Kamano Yoshiaki

  Faculty of Science, Kanagawa University

• Yamashita Ayano

  Faculty of Science, Kanagawa University

• Takeuchi Hiroaki

  Faculty of Science, Kanagawa University

• Kohyama Koichi

  Faculty of Science, Kanagawa University

• Nogawa Toshihiko

  Faculty of Science, Kanagawa University

• Kohyama Koichi

  Faculty Of Science Kanagawa University

• Kamano Yoshiaki

  Faculty Of Science Kanagawa University

• Yamashita Ayano

  Faculty Of Science Kanagawa University

• Nogawa Toshihiko

  Faculty Of Science Kanagawa University

• Takeuchi Hiroaki

  Faculty Of Science Kanagawa University

• Takeuchi Hiroaki

  Faculty Of Engineering Osaka University

• 山下 文乃

  Faculty of Science, Kanagawa University

• 野川 俊彦

  Cancer Research Institute and Department of Chemistry, Arizona State University

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