Practical Synthesis of the Disaccharide Epitope, D-Galactopyranosyl-α-1,3-D-galactopyranose, by using 1,2 ; 5,6-Di-O-cyclohexylidene-α-D-galactofuranose as the Glycosyl Acceptor

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概要

• 論文の詳細を見る

• D-Galactosyl-α-1,3-D-galactopyranose (1) was chemically prepared in a good yield by coupling phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside (5) or 2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl bromide (8) with 1,2 : 5,6-di-O-cyclohexylidene-α-D-galactofuranose (3) with subsequent de-O-benzylation and de-O-cyclohexylidenation of the resulting protected α-1,3-disaccharide.

• 社団法人日本農芸化学会の論文
• 2000-09-23

著者

• OHRUI Hiroshi

  Division of Applied Life Science, Graduate School of Agricultural Science, Tohoku University

• Sakamoto Isao

  Division Of Life Science Graduate School Of Agricultural Science Tohoku University

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• Practical Synthesis of the Disaccharide Epitope, D-Galactopyranosyl-α-1,3-D-galactopyranose, by using 1,2 ; 5,6-Di-O-cyclohexylidene-α-D-galactofuranose as the Glycosyl Acceptor
• Development of phosphine reagents for the high-performance liquid chromatographic-fluorometric determination of lipid hydroperoxides

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