On the Magic of Microwave-assisted Organic Synthesis : 1,5-Benzodiazepin-2-one from o-Phenylenediamine and Ethyl Acetoacetate

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概要

• 論文の詳細を見る

• Microwave-assisted synthesis of 4-methyl-2,3-dihydro-1H-1,5-benzodiazepin-2-one by the condensation of 1,2-phenylenediamine and ethyl acetoacetate was examined. The yields were compared with those by classical heating under various conditions. The yield is mainly determined by the temperature of the reaction mixtures, and little affected by the difference in the heating methods. Nonthermal effects in microwave heating have not been observed.

• Chemical Society of Japanの論文
• 2006-12-05

著者

• Itoh Yuki

  Division Of Materials Chemistry Graduate School Of Engineering Hokkaido University

• KOIZUMI Hitoshi

  Division of Materials Chemistry, Graduate School of Engineering, Hokkaido University

• ICHIKAWA Tsuneki

  Division of Materials Chemistry, Graduate School of Engineering, Hokkaido University

• Koizumi Hitoshi

  Division Of Materials Chemistry Graduate School Of Engineering Hokkaido University

• Itoh Y

  Division Of Materials Chemistry Graduate School Of Engineering Hokkaido University

• Ichikawa Tsuneki

  Division Of Materials Chemistry Graduate School Of Engineering Hokkaido University

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