Study on the Determination of Toxic Chemicals in Exhaust Gas (II). o-Chloronitrobenzene, m-Chloronitrobenzene, p-Chloronitrobenzene.:—<I>o</I>-Chloronitrobenzene, <I>m</I>-Chloronitrobenzene, <I>p</I>-Chloronitrobenzene—
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概要
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A new method for the determination of ο-, m-, ρ-chloronitrobenzenes (CNBs) in exhaust gas was developed. The method was applicable to the analysis of CNBs in gas samples containing up to 30% of water. CNBs were collected with SEP PAK<SUP>®</SUP>PS2 cartridge after conditioning with η-hexane. CNBs were eluted with n-hexane and determined by capillary gas chromatography-mass spectrometry (GC/MS) and gas chromatography using flame thermoionic detector (GC/FTID) .<BR>Detection limits, relative standard deviations and recoveries of CNBs were 28.1-46.2 μg/m<SUP>3</SUP>, 3.62-8.94%, 85.6.95.0% in GC/MS and 155-200 μg/m<SUP>3</SUP>, 3.9-25.4%, 78.7-98.6% in GC/FTID.
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