Particle Formation by CO2 Laser-Induced Breakdown (III). The Formation of Mo and MoS2 Fine Powders from Mo(CO)6.
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Fine powdered Mo and MoS<SUB>2</SUB> were synthesized in vapor phase reactions by a TEA-CO<SUB>2</SUB>laser-induced breakdown technique. Molybdenum particles were prepared from Mo (CO)<SUB>6</SUB>; molybdenum sulfide particles were prepared from a mixture of Mo (CO)<SUB>6</SUB> and CS<SUB>2</SUB>. The particulatem aterials were characterized by scanning electron microscopy, ICP ctomic emission spectroscopy, and X-ray diffraction. The particles are monodispersed, neafly sphedcal, and 0.05-0.4μm indiameter. An X-ray diffraction study indicates that the Mo particle is crystalline and MoS<SUB>2</SUB>particle is amorphous. The yield of the Mo particle increased linearly with increasing laser pulseenergy.
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社団法人 レーザー学会 | 論文
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