A simple pressurized high-temperature proton NMR apparatus for the thermal degradation of polymers.

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概要

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• A simple pressurized, externally heated, high-temperature proton NMR apparatus for the temperature range from 293 to 823 K and pressure range from 0.1 to 40 MPa is reported. The sample cell has a capillary opening and the vessel is pressurized by inert gas. An application of this apparatus to the thermal degradation of poly(vinyl chloride) is presented.

• 公益社団法人 日本化学会の論文

著者

• Shimokawa Shigezo

  Nmr Laboratory Faculty Of Engineering Hokkaido University

• Makino Kazuo

  Department of Applied Chemistry, Faculty of Engineering, Hokkaido University

• Yamada Eiji

  NMR Laboratory, Faculty of Engineering, Hokkaido University

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• A simple pressurized high-temperature proton NMR apparatus for the thermal degradation of polymers.

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