Simultaneous determination of trace amounts of carbazole and anthracene in dibenzofuran by synchronous fluorescence spectrometry after zone-melting separation.
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概要
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Trace amounts of carbazole and anthracene in dibenzofuran can be simultaneously determined by measuring the synchronous fluorescence intensities at 336 and 381 nm respectively. The determination limit is 2 ppm. For the application of this method to the practical samples containing interfering impurities, a zone-melting technique was applied successfully to remove the impurities prior to the determination. The recoveries of carbazole and anthracene were 99 and 92% respectively.
- 公益社団法人 日本化学会の論文
著者
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Tachibana Masaki
Faculty of Engineering, Yamanashi University
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Furusawa Motohisa
Faculty of Engineering, Yamanashi University
関連論文
- Simultaneous determination of trace amounts of carbazole and anthracene in dibenzofuran by synchronous fluorescence spectrometry after zone-melting separation.
- Zone-melting separation of carbazole and anthracene from polynuclear aromatic compounds using biphenyl as a medium, followed by the synchronous fluorometric determination.
- The separation by means of the zone-melting technique and the spectrofluorometric determination of trace amounts of anthracene in phenanthrene.