Synthesis of guanidino-1,3,5-triazines using DMF.

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概要

• 論文の詳細を見る

• 2,4,6-Triguanidino-1,3,5-triazine and 2,4,6-tris(3-methylguanidino)-1,3,5-triazine were synthesized in 42 and 52% yields, respectively, by the cyclotrimerization of cyanoguanidine and 1-methyl-3-cyanoguanidine using DMF as a solvent in the presence of hydrogen chloride. 1-Phenyl-3-cyanoguanidine, 1,2-dimethyl-3-cyanoguanidine, and 2-imidazolidinylidenecyanamide, however, were cyclodimerized to the corresponding guanidino-1,3,5-triazines in a similar manner.

• 公益社団法人 日本化学会の論文

著者

• Iio Kokoro

  Industrial Products Research Institute

• Ichikawa Eiichi

  Faculty of Engineering, Tokyo Institute of Technology

関連論文

• The preparation of 1-carbamoyl-3-cyanoguanidine and 1-cyanobiuret from cyanourea.
• Synthesis of guanidino-1,3,5-triazines using DMF.

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