One pot synthesis of dinuclear tungsten(V) compounds containing [W2XY(.MU.-S)2]2+ (X=O, S; Y=O, S) cores by thermally induced internal electron-transfer processes.

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概要

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• New synthetic methods for the preparation of dimeric tungsten(V) complexes are described containing the core [W<SUB>2</SUB>XY(μ-S)<SUB>2</SUB>]<SUP>2+</SUP> (X=O,S; Y=O,S). The synthesized complexes have been characterized by a variety of spectroscopic techniques. [W<SUB>2</SUB>OS(μ-S)<SUB>2</SUB>(S<SUB>2</SUB>CNEt<SUB>2</SUB>)<SUB>2</SUB>] has been found to react with cyanide to give [W<SUB>2</SUB>O<SUB>2</SUB>(μ-S)<SUB>2</SUB>(S<SUB>2</SUB>CNEt<SUB>2</SUB>)<SUB>2</SUB>].

• 公益社団法人 日本化学会の論文

著者

• Sarkar Sabyasachi

  Department Of Chemical Engineering University Of Nebraska

• Ansari Mohammad

  Department of Chemistry, Indian Institute of Technology

• Chandrasekaran Jayanthi

  Department of Chemistry, Indian Institute of Technology

• Sarkar Sabyasachi

  Department of Chemistry, Indian Institute of Technology

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• One pot synthesis of dinuclear tungsten(V) compounds containing [W2XY(.MU.-S)2]2+ (X=O, S; Y=O, S) cores by thermally induced internal electron-transfer processes.
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