The selective protection of uridine with a p-methoxybenzyl chloride: A synthesis of 2'-O-methyluridine.

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概要

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• 2′-<I>O</I>-Methyluridine was prepared through 5 steps from uridine by use of <I>p</I>-methoxybenzyl group (PMB) as an N<SUP>3</SUP>-protecting group of uridine. A chemoselective protection method has been developed by use of DBU as a base and deprotection was effected by AlCl<SUB>3</SUB>–anisole system.

• 公益社団法人 日本化学会の論文

著者

• Nishimoto Hiroyuki

  Department of Resources Chemistry, Faculty of Engineering, Ehime University

• Akiyama Takahiko

  Department of Resources Chemistry, Faculty of Engineering, Ehime University

関連論文

• The selective protection of uridine with a p-methoxybenzyl chloride: A synthesis of 2'-O-methyluridine.

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