Alkoxysilanes. VII. The Preparation of Alkylalkoxysiloxanes

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概要

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• Trimethylsiloxytri-<I>t</I>-butoxysilane (I), bis(trimethylsiloxy)di-<I>t</I>-butoxysilane (II), and bis(trimethylsiloxy)bis(tri-<I>t</I>-butoxysiloxy)silane (III) were prepared by the reaction of trimethylchlorosilane with tri-<I>t</I>-butoxysilanol, di-<I>t</I>-butoxysilanediol, and bis(tri-<I>t</I>-butoxysiloxy)silanediol respectively. Bis(tri-<I>t</I>-butoxysiloxy)dimethylsilane (IV) was also obtained by the reaction of dimethyldichlorosilane with tri-<I>t</I>-butoxysilanol. The reaction of dimethyldichlorosilane with di-<I>t</I>-butoxysilanediol or bis(tri-<I>t</I>-butoxysiloxy)silanediol gave tetramethyltetra-<I>t</I>-butoxy (V) or tetramethyltetra(tri-<I>t</I>-butoxysiloxy)cyclooctasiloxane (VI). These compounds were identified by means of elemental analysis, molecular-weight determination, and a study of the IR and NMR spectra.

• 公益社団法人 日本化学会の論文

著者

• Okuda Keisuke

  Department of Industrial Chemistry, Faculty of Engineering, Science University of Tokyo

関連論文

• Total Electron Scattering Cross Sections for Simple Perfluorocarbons (Atomic and Molecular Physics)
• Alkoxysilanes. VII. The Preparation of Alkylalkoxysiloxanes

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