Enzymatic Synthesis of Palm Olein-based Fatty Thiohydroxamic Acids
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概要
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Fatty thiohydroxamic acids (FTAs) have been successfully synthesized from palm olein and thiohydroxamic acid by a one-step lipase catalyzed reaction. The use of immobilized lipase (Lipozyme RMIM) as the catalyst for the preparation reaction provides an easy isolation of the enzyme from the products and other components in the reaction mixture. The FTAs were characterized using Fourier transform infrared (FTIR) spectroscopy, proton nuclear magnetic resonance (1H NMR) technique and elemental analysis. The highest conversion percentage (95 %) was obtained when the process was carried out for 30 hours using urea to palm oil ratio of 6.0: 1.0 at 40 °C. The method employed offers several advantages such as renewable and abundant of the raw material, simple reaction procedure, environmentally friendly process and high yield of the product.
- 日本油化学会の論文
著者
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Al-Mulla Emad
Department of Chemistry, Faculty of Science, University Putra Malaysia
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Yunus Wan
Department of Chemistry, Faculty of Science, University Putra Malaysia
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Ibrahim Nor
Department of Chemistry, Faculty of Science, University Putra Malaysia
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Rahman Mohd
Department of Chemistry, Faculty of Science, University Putra Malaysia
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Rahman Mohd
Department Of Chemistry Faculty Of Science Universiti Putra Malaysia
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Al-Mulla Emad
Department of Chemistry, College of Science, University of Kufa
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Ibrahim Nor
Department of Chemistry, Faculty of Science, Universiti Putra Malaysia
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Yunus Wan
Department of Chemistry, Faculty of Science, Universiti Putra Malaysia
関連論文
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