Preparation of porous biphasic β-TCP/HA bioceramics with a natural trabecular structure from calcined cancellous bovine bone
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概要
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Porous biphasic β-TCP/HA bioceramics were fabricated by sintering of calcined cancellous bovine bone (CBB) treated with different quantities of NH4H2PO4 at various temperatures. The obtained materials had a porous structure (macropores within 200-800 μm and micropores within 1-5 μm) of natural trabecular bones. The specimens were characterized by X-ray diffraction, scanning electron microscopy (SEM), and gravimetric thermal analysis (TG). The results revealed that porous biphasic β-TCP/HA bioceramics were successfully prepared at sintering temperatures within 762°C-829°C. Biological apatite of calcined CBB was found to transform partly into Ca2P2O7 at heating temperatures between 503°C and 762°C. As the ratio NH4H2PO4/calcined-CBB increased, bioceramics with different phase compositions of β-TCP/HA, β-TCP/HA/Ca2P2O7 or β-TCP/Ca2P2O7 were produced after sintering.
著者
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JIN Hai-Bo
School of Materials Science and Engineering, Beijing Institute of Technology
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GUO Chao-Bang
School of Materials Science and Engineering, Beijing Institute of Technology
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MAO Ke-Ya
Department of Orthopedic Surgery, General Hospital of PLA
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DOROZHKIN Sergey
Kudrinskaja sq.
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AGATHOPOULOS Simeon
Department of Materials Science and Engineering, University of Ioannina
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Jin Hai-bo
School Of Material Sci. And Engineering Beijing Inst. Of Technol.
関連論文
- Preparation of porous biphasic β-TCP/HA bioceramics with a natural trabecular structure from calcined cancellous bovine bone
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