Synthesis of Di- and Tri-saccharides Having the Sequences [β-D-GlcNAc]n (1→X)-α-D-Man in the Glycan of glycopeptides
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概要
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Five model di- and tri-saccharides corresponding to the part structures of the glycan of glycopeptides were synthesized with regio- and stereo-control. They were as follows: methyl 3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-α-D-mannopyranoside, methyl 4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-α-D-mannopyranoside, methyl 6-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-α-D-mannopyranoside, methyl 3, 6-di-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-α-D-mannopyranoside, and methyl 2, 4-di-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-α-D-mannopyranoside. Some aspects of 1H- and 13C-NMR data of these synthetic saccharides were also described.
- 社団法人 日本農芸化学会の論文
著者
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Ogawa Tomoya
The Institute Of Physical And Chemical Research
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NAKABAYASHI Satoru
The Institute of Physical and Chemical Research
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