Pre-activation of fully acetylated dodecyl thioglycosides with BSP-Tf2O led to efficient glycosylation at low temperature
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Fully acetylated dodecyl thioglycosides found to be used as glycosyl donors by activation with 1.benzenesulfinyl piperidine (BSP) and triflic anhydride (Tf2O) at -78℃, and the glycosyl acceptor was added to the reaction mixture at the same temperature to furnish various disaccharides and Lewis a (Le^a) trisaccharide in good yields.
- Elsevierの論文
- 2009-02-17
Elsevier | 論文
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