COOL-STAGE AFM, A NEW AFM METHOD FOR IN SITU OBSERVATIONS OF MINERAL GROWTH AND DISSOLUTION AT REDUCED TEMPERATURE : INVESTIGATION OF THE RESPONSIVENESS AND ACCURACY OF THE COOLING SYSTEM AND A PRELIMINARY EXPERIMENT ON BARITE GROWTH
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概要
- 論文の詳細を見る
Using in situ cool-stage atomic force microscopy (AFM), we can observe sample surfaces in air or fluid directly at the site or step level at low or reduced temperatures (〜-35℃ in air or 〜4℃ in fluid). The main components of the new AFM system include a heater/cooler element (cool-stage), specialized heater/cooler piezoelectric scanner with a heat exchanger, Thermal Applications Controller, AFM fluid cell, and fluid cooling system to cool the piezo scanner. We investigate the responsiveness and accuracy of the temperature control in the cooling AFM system by varying the setpoint temperature of the cool-stage and flow rate of the water flowing through the AFM fluid cell and thereby obtain suitable experimental conditions for in situ cool-stage AFM observations of mineral growth and dissolution in aqueous solutions at low or reduced temperatures. We also report the results of a preliminary experiment on in situ observations of the growth behavior on the barite (001) surface in a supersaturated BaSO_4 solution at reduced temperature (25℃ to 15℃) using the new AFM method.
- 日本粘土学会の論文
- 2012-12-00
著者
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NAKAMUTA Yoshihiro
Kyushu University
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Ishida Kiyotaka
Department Of Evolution Of Earth Environments Graduate School Of Social And Cultural Studies Kyushu
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Kuwahara Yoshihiro
Department Of Applied Chemistry Faculty Of Engineering Osaka University
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Fujii Rie
Department Of Materials Science Tokai University
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Hayashi Tatsuya
Department Of Biochemistry Mie Prefectural College Of Nursing
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Uehara Seiichiro
Department Of Earth And Planetary Sciences Faculty Of Science Kyushu University
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NAKAMUTA YOSHIHIRO
Kyushu University Museum, Kyushu University
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KITA ITSURO
Department of Environmental Changes, Faculty of Social and Cultural Studies, Kyushu University
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FUJII RIE
Department of Geology and Mineralogy, Division of Earth and Planetary Sciences, Graduate School of Science
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HAYASHI TATSUYA
Department of Geology and Paleontology, National Museum of Nature and Science:(Present office)Mifune Dinosaur Museum
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KUWAHARA YOSHIHIRO
Department of Environmental Changes, Faculty of Social and Cultural Studies, Kyushu University
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