High-Performance Liquid Chromatographic Determination of Ustiloxin A in Forage Rice Silage(Toxicology)

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概要

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• We describe a high-performance liquid chromatographic method for determining ustiloxin A, a mycotoxin produced by Ustilaginoidea virens, in forage rice silage. Lyophilized silage samples were ground and extracted with water. The extracts were purified by solid-phase extraction and subjected to high-performance liquid chromatography using an octadecylsilane-bonded column. Separated ustiloxin A was detected with ultraviolet (UV) absorption at 254nm. The limit of quantitation for ustiloxin A in silage found to be 2.5mg/kg. The present method can be used for routine monitoring of the contamination of ustiloxin A in forage rice silage.

• 2009-02-25

著者

• Matsumoto Yuichi

  Safety Research Team National Institute Of Animal Health:fukushima Kenchu Livestock Hygiene Service

• Miyazaki Shigeru

  Safety Research Team National Institute Of Animal Health

• UCHIHARA Tsutomu

  Safety Research Team, National Institute of Animal Health

• MORIMOTO Kazuhide

  Livestock Technology Research Center, Hiroshima Prefectural Technology Research Institute

• Uchihara Tsutomu

  Safety Research Team National Institute Of Animal Health:okinawa Institute Of Animal Health

• Morimoto Kazuhide

  Livestock Technology Research Center Hiroshima Prefectural Technology Research Institute

関連論文

• The Effects of Acute Exposure to Deoxynivalenol on Some Inflammatory Parameters in Miniature Pigs
• High-Performance Liquid Chromatographic Determination of Ustiloxin A in Forage Rice Silage(Toxicology)
• Effects of Feeding Calves Genetically Modified Corn Bt11: A Clinico-Biochemical Study
• Safety Evaluation of Bt Plants

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