N-Trifluoroacetyl-L-prolyl Amino Acid n-Butyl Ester Derivatives for the Ultramicrodetermination of Amino Acids by Mass Fragmentography

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概要

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• The fragmentation of 46 kinds of N-trifluoroacetyl-L-prolyl amino acid n-butyl esters upon electron impact is investigated for the ultramicrodetermination of amino acids by mass fragmentography. It is found that ion at m/e 166 is the common and base peak for most of the amino acid. Characteristic ions for each α-amino acid are observed at m/e (M-101) or (R+29). Using mass fragmentography monitored at m/e 166,about 10^<-10> g of amino acids can be detected.

• 公益社団法人日本薬学会の論文
• 1977-02-25

著者

• 村井 朝夫

  Central Research Laboratories Ajinomoto Co. Inc.

• 岩瀬 廣

  Central Research Laboratories Ajinomoto Co. Inc.

関連論文

• Resolution of Racemic Amino Acids by Gas Chromatography. II. N-Perfluoroacyl-L-prolyl Derivatives
• Resolution of Racemic Amino Acids by Gas Chromatography. I. N-Trifluoroacetyl-L-prolyl Derivatives
• Gas Chromatography-Mass Spectrometry of Trimethylsilyl Derivatives of Amino Acids
• Gas Chromatography-Mass Spectrometry of Trimethylsilyl Derivatives of Amines
• On the Derivatives for the Ultramicrodetermination of Amines by Mass Fragmentography
• N-Trifluoroacetyl-L-prolylamine Derivatives for the Ultramicrodetermination of Amines by Mass Fragmentography
• N-Trifluoroacetyl-L-prolyl Amino Acid n-Butyl Ester Derivatives for the Ultramicrodetermination of Amino Acids by Mass Fragmentography

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