Caffeic Acid Phenethyl Ester(CAPE) : Synthesis and X-Ray Crystallographic Analysis

スポンサーリンク

概要

• 論文の詳細を見る

• The structure of caffeic acid phenethyl ester[2-propenoic acid, 3-(3, 4-dihydroxyphenyl)-, 2-phenethyl ester](I), C_<17>H_<16>O_4・1/2C_6H_6, synthesized by base-catalyzed alkylation of caffeic acid salt with β-bromoethylbenzane in HMPA(hexamethylphosphoramide) and recrystallized from benzene, was confirmed by single crystal X-ray diffraction. The crystals are triclinic, space group P1, Z=2, unit cell dimension a=5.8129(9)Å, b=11.122(2)Å, c=13.226(2)Å, α=97.080(3)°, β=101.467(3)°, γ=95.405(3)°, V=825.4(2)Å^3, D_<calc>=1.301g/cm^3, F(000)=342. The packing of the molecule is stabilized by intermolecular O_1H…O_4(2.69Å)and O_1…HO_2(2.82Å)hydrogen bonds.

• 公益社団法人日本薬学会の論文
• 2001-02-01

著者

• Son Sopheak

  Department Of Food Science Cornell University

• Lewis Betty

  Division Of Nutritional Sciences Cornell University

• LOBKOWSKY Emil

  Department of Chemistry and Chemical Biology, Cornell University

• Lobkowsky Emil

  Department Of Chemistry And Chemical Biology Cornell University

• Son Soheak

  Department of Food Science, Cornell University

関連論文

• Caffeic Acid Phenethyl Ester(CAPE) : Synthesis and X-Ray Crystallographic Analysis

スポンサーリンク