Estimated and Evaluated Residual Stress by Vickers Indentation in Several Structural Ceramics

概要

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Residual stress was generated in several structural ceramics by sintering and grinding, then estimated using the Vickers indentation method. First, we sought the most appropriate pretreatment for measuring fracture toughness (basis value, K_C), while preventing any influence from residual stress. This is important in estimating residual stress using the Vickers indentation method. Based on that value, the residual stress in Al_2O_3 and Si_3N_4 ceramics was estimated by the Vickers indentation method. Next, several problems in using the indentation method on ZrO_2 ceramics were discussed, focusing on phase transformation. Residual stress in Al_2O_3 and Si_3N_4 was nearly eliminated by annealing the specimen after hand grinding. Consequently, this treatment method is considered effective for determining the basis value K_C. The estimated residual stress value in Al_2O_3 and Si_3N_4 obtained by the Vickers indentation method at 98N corresponded closely to the values obtained by the X-ray method. The value for ZrO_2, however, was larger than that found by the X-ray method. This difference is assumed to derive from phase transformation.
社団法人日本材料学会の論文
2003-03-15