A Sandwich Cubane-Type Mo-Sn Cluster. Synthesis and Crystal Structure of [(HO2O)9Mo3OS3SnS3OMo3(HO2O)9](CH3C6H4SO3)8 18H2O.
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A novel sandwich cubane-type mixed-metal Mo–Sn cluster compound [Mo<SUB>6</SUB>SnO<SUB>2</SUB>S<SUB>6</SUB>(H<SUB>2</SUB>O)<SUB>18</SUB>](pts)<SUB>8</SUB>·18H<SUB>2</SUB>O (A) was synthesized by the reaction of [Mo<SUB>3</SUB>(µ<SUB>3</SUB>-S)(µ-O)(µ-S)<SUB>2</SUB>(H<SUB>2</SUB>O)<SUB>9</SUB>]<SUP>4+</SUP> (B) with tin metal in <I>p</I>-toluensulphonic acid (Hpts) solution. The compound A was characterized by the X-ray structure determination and UV–vis spectrum.
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公益社団法人 日本化学会 | 論文
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