Research on Fabrication Conditions of TiO2 Pillared Porous Manganese Oxide Nanocompound
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概要
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TiO<SUB>2</SUB> pillared porous manganese oxide nanocompound with high TiO<SUB>2</SUB> amount was successfully synthesized from birnessite (H) -type manganese oxide (H-BirMO) by intercalation of alkylamine followed by solvothermal treatment in pure titanium isopropoxide (TIIP) liquid. The effects of solvothermal treatment temperatures and chain length of preintercalated alkylamine molecules to the pillared structure were systematically investigated. The structural evolution of TiO<SUB>2</SUB> pillared porous manganese oxide nanocompound was characterized by XRD, SEM, N<SUB>2</SUB> adsorption-desorption and element analysis. The amount of intercalated TiO<SUB>2</SUB> depends on the solvothermal treatment temperatures and the water amount in samples and not connect with the basal spacing of samples. TiO<SUB>2</SUB> pillared porous manganese oxide nanocompound with high TiO<SUB>2</SUB> amount had a BET surface area of 114 m<SUP>2</SUP>/g with a galley height of about 1.76 nm between layers.
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