Preparation of New Functionalized Graft Polymers and Their Application as Supports in Organic Synthesis
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概要
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New functionalized graft polymers (fCMS-Br<SUB>3</SUB>, fCMS-BH<SUB>4</SUB>) were synthesized from an anion-exchange fiber, which was prepared using radiation-induced graft polymerization. The abilities of these polymers as polymer-supported reagents are discussed. After bromination of <I>p</I>-cresol and reduction of benzaldehyde with these polymers in a column-mode, the relationship between flow rate and product yield was examined, and compared with the results of the polymer-supported reagents prepared from a porous resin. In both cases, the present graft polymers provided the desired compounds more efficiently even at a high flow rate.
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