Phase Transition and Effect of Small Amount of Water Included in K2ZnCl4 Crystal.
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概要
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Absorption/desorption of small amount of water and its effects on the phase transition at 146K in K2ZnCl4 were studies by FT-IR spectroscopy and adiabatic calorimetry. Existence of water molecule in absorbed crystal was substantiated by FT-IR spectra. It was verified by heat capacity measurements on single crystals of large size that the water is absorbed in the crystal. The reproducibility and reversibility of the absorption/desorption were confirmed by repeating heat/ventilation treatment and exposure of the sample to the laboratory atmosphere.
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