Crystal Structure of Bis(nitrosocyclohexane)

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概要

• 論文の詳細を見る

• The crystal structure of bis(nitrosocyclohexane), (C<SUB>6</SUB>H<SUB>11</SUB>NO)<SUB>2</SUB>, has been determined by means of three-dimensional X-ray analysis by the photographic method. The crystal belongs to the triclinic space group <I>P</I> \bar1, with cell parameters, <I>a</I>=10.133 A, <I>b</I>=6.758 A, <I>c</I>=5.583 A, α=121°42′, β=96°50′, γ=78°06′. The unit cell contains one molecule. The nitrogen and oxygen atoms and the carbon atoms bound to nitroso-groups, CNO–O′N′C′, are almost coplanar, and the oxygen atoms take a trans configuration around the N–N′ bond. The cyclohexane ring takes a chair form and the nitrogen atom is bound to an equatorial bond. The CNO-O′N′C′ plane is twisted from the cyclohexane ring by 73°.

• 公益社団法人 日本化学会の論文

著者

• Kashiwagi Michio

  Basic Research Laboratories Toyo Rayon Company Ltd.

• Tanimura Masamitsu

  Basic Research Laboratory, Toray Industries Inc.

• Tanimura Masamitsu

  Basic Research Laboratories, Toray Industries, Inc.

• Kobori Kiyotomi

  Basic Research Laboratory, Toray Industries Inc.

• Kinoshita Yukio

  Basic Research Laboratory, Toray Industries Inc.

• Kobori Kiyotomi

  Basic Research Laboratories, Toray Industries, Inc.

• Kashiwagi Michio

  Basic Research Laboratory, Toray Industries Inc.

• Kashiwagi Michio

  Basic Reseach Laboratories, Toray Industries, Inc.

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