Isolation and circular dichroism of the isomers of dicyanobis((R,R)-1,2-cyclohexanediamine) and bis((S)-propylenediamine)cobalt(III) complexes.
スポンサーリンク
概要
- 論文の詳細を見る
Three isomers of <I>trans</I>- and <I>cis</I>-[Co(CN)<SUB>2</SUB>{(<I>R</I>,<I>R</I>)-1,2-cyclohexanediamine}<SUB>2</SUB>]<SUP>+</SUP> and five isomers of the corresponding (<I>S</I>)-propylenediamine complexes have been isolated by chromatography with Dowex 50W-X8 and SP-Sephadex columns, their geometrical structures being assigned on the basis of the ligand field absorption and PMR spectra. Isomers of <I>cis</I>-[Co(CN)<SUB>2</SUB>{(<I>S</I>)-propylenediamine}<SUB>2</SUB>]Cl, which have different placement of methyl groups of (<I>S</I>) -propylenediamine, gave different methyl PMR resonances with different chemical shifts. The absolute configuration of the isomers was determined from the circular dichroism in the first spin-allowed d-d and the charge transfer band region. The configurational and the vicinal effect have been discussed.
- 公益社団法人 日本化学会の論文
著者
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Nishikawa Hiroaki
Department Of Cardiology Faculty Of Medicine Fukuoka University
-
Saito Kazuo
Department Chemistry Faculty Of Science Tohoku University
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Shibata Muraji
Department of Chemistry Faculty of Science Kanazawa University
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Yamanaka Toshimasa
Department of Chemistry, Faculty of Science, Tohoku University
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Hamada Nobuhiro
Department of Chemistry, Faculty of Science, Kanazawa University
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Komatsu Naoto
Department of Chemistry, Faculty of Science, Kanazawa University
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