速中性子放射化法による金属チタン中の酸素の定量
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The oxygen content of titanium metal was determined by bombarding samples with 14 MeV neutrons from a Cockcroft-Walton machine and measuring the 7.35 second nitrogen-16 gamma activity produced by the reaction <SUP>16</SUP>O(<I>n</I>, <I>p</I>)<SUP>16</SUP>N. In this paper, optimum condition for the measurement of gamma rays of <SUP>16</SUP>N, a correction for the absorption of gamma-rays by samples are discussed. The analytical results by this method are in good agreement with those by the vacuum fusion method. The sensitivity for oxygen is about 1000 counts/mg of oxygen and the standard deviation of the method at the level of oxygen concentration 0.1% is 4%.<BR>This method may be used to study the accuracy and the precision of the conventional method because the method is non-destructive.
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