Preparation of Anodised Aluminium Catalysts by an Electrolysis Supporting Method for VOC Catalytic Combustion
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概要
- 論文の詳細を見る
Catalytic combustion of volatile organic compounds (VOCs) benefits from a low oxidation temperature due to less energy consumption. It is widely applied in industry. A novel technique of Pt/Al2O3/Al catalyst preparation is presented in this paper. Al2O3 film was formed on an Al plate by anodic oxidation in 4% oxalic acid solution at 50 A·m–2 current density. After anodic oxidation, Pt was supported on the oxidized plate utilizing an electrolysis supporting method with an alternating current in an aqueous solution of chloroplatinic acid hexahydrate under both high and low voltages. Catalytic activity was evaluated by both toluene and benzene combustion. Dispersion of platinum in developed catalysts was about 20%, measured by CO pulse adsorption.In the activity test, toluene or benzene was mixed with air and then toluene–air and benzene–air mixtures combusted on the developed catalysts. It is shown that a catalyst prepared under a high voltage has a higher reaction rate than that one prepared under low voltage. This may be explained by that large platinum particles were formed on the film by high voltage. In the running time of 140 hours duration, there exists an induction process of about 10 hours for fresh catalysts, in which, the conversion of toluene was promoted by up to about 8%, and with no obvious change in the reactions that follow. Experimental results indicated that electrolysis impregnation can be regarded as a short-time supporting method for preparing catalyst.
- 社団法人 化学工学会の論文
- 2005-02-01
著者
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SUZUKI Koji
Department of Public Health, Fujita Health University School of Health Sciences
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亀山 秀雄
東京農工大学
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SAKURAI Makoto
Department of Chemical Engineering, Tokyo University of Agriculture and Technology
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KAMEYAMA Hideo
Department of Chemical Engineering, Tokyo University of Agriculture and Technology
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Wang Lifeng
Department Of Chemical Engineering Faculty Of Engineering Tokyo University Of Agriculture And Techno
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Wang L
Department Of Chemical Engineering Tokyo University Of Agriculture And Technology
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Kameyama Hideo
Department Of Chemical Engineering Faculty Of Engineering Tokyo University Of Agriculture And Techno
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Suzuki Koji
Department Of Public Health Fujita Health University Of Health Sciences
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VIEN Vo
Department of Chemical Engineering, Faculty of Engineering, Tokyo University of Agriculture and Tech
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Vien Vo
Department Of Chemical Engineering Faculty Of Engineering Tokyo University Of Agriculture And Techno
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Sakurai Makoto
Department Of Cardiovascular Surgery Osaka Medical Center For Cancer And Cardiovascular Diseases
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Sakurai M
Department Of Chemical Engineering Faculty Of Engineering Tokyo University Of Agriculture And Techno
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Sakurai Makoto
Department Of Applied Chemistry College Of Engineering Chubu University
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Suzuki Koji
Department Of Applied Chemistry Faculty Of Science And Technology Keio University
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Suzuki Koji
Department Of Chemical Engineering Faculty Of Engineering Tokyo University Of Agriculture And Techno
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SUZUKI Koji
Department of Agricultural Chemistry, University of the Ryukyus
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