Headspace solid-phase micro-extraction and gas chromatography with micro-electron capture detection for the measurement of p,p'-DDE in rat whole blood and hair
スポンサーリンク
概要
- 論文の詳細を見る
A sensitive, specific, and reproducible capillary gas chromatography (GC) with micro-electron capture detection (μ-ECD) method using headspace solid-phase micro-extraction (HS-SPME) for the quantitative analysis of p,p'-DDE in rat whole blood and hair was developed. A 100 μm polydimethylsiloxane (PDMS) phase was used for the extraction. The obtained detection limits were 0.003ng/nig and 0.004ng/mg in whole blood and hair, respectively, at a signal-to-noise ratio of 3 (S/N=3). Linearity was obtained in the ranges 0.003-2.0ng/mg and 0.004-2.0ng/mg in whole blood and hair, respectively, and the correlation coefficients of whole blood and hair were greater than 0.998. This method was successfully applied to the analysis of p,p'-DDE in rat whole blood and rat hair after an oral dose of p,p'-DDE.
- 東海大学の論文
著者
-
SAITO Takeshi
Department of Surgery, Funabashi Municipal Medical Center
-
TAKEICHI Sanae
Department of Forensic Medicine, Tokai University School of Medicine
-
KUSAKABE Takahiko
Department of Forensic Medicine, Tokai University School of Medicine
-
Saito Takeshi
Department Of Forensic Medicine Tokai University School Of Medicine
-
Saito T
Tokai Univ. School Of Medicine
-
Saito Takuro
Department Of Forensic Medicine Tokai University School Of Medicine
-
Takeichi Sanae
Department Of Forensic Medicine Tokai University School Of Medicine
-
Saito T
Department Of Forensic Medicine Tokai University School Of Medicine
-
Kusakabe Takahiko
Department Of Forensic Medicine Tokai University School Of Medicine
-
Saito Takeshi
Department Of Cardiovascular Surgery Sendai Open Hospital
-
Saito Takeshi
Department of Applied Physics, Hokkaido University, Kita-13, Nishi-8, Kita-ku, Sapporo 060, Japan
関連論文
- Analyse Micro-Locale $\ell$-Adique en Caracteristique${p}$>0 le Cas d'un Trait
- A Case of Breast Cancer Metastatic to the Tail of the Pancreas
- ヒトモデルとしてのブタにおけるTLRファミリーの解析と乳業界における発展的利用性
- Bacteriocin production of probiotic Lactobacillus gasseri LA39 isolated from human feces in milk-based media
- Development of molecular immunoassay system for probiotics via toll-like receptors based on food immunology
- 国際学会報告 第4回アジア乳酸菌会議および第3回乳酸菌と健康に関する国際シンポジウムに参加して
- ヒトABO式血液型を認識する乳酸菌の発見とその利用 : プロバイオティック乳酸菌の複雑な腸管付着性機構の一端を解明
- Studies on the Ventricular Asynchronism in Right Bundle Branch Block
- Monolithic Spin-column Extraction and GC-MS Method for the Assay of Eperisone in Human Serum
- IS O-16 The expression of biliary transporters in biliary atresia(International Session 3 Chest and Others,Science and Art for Sick Children)
- IS O-03 123I-MIBG-navigated surgery in neuroblastoma(International Session 1 Neuroblastoma,Science and Art for Sick Children)
- Plasma triglyceride-rich lipoprotein remnants as a risk factor of 'Pokkuri disease'
- Familial Type V Hyperlipoproteinemia with Hyper-Remnant-Like Particle-Cholesterol Accompanied with Apolipoprotein E3/E4 Phenotype
- A New Approach for the Detection of Type III Hyperlipoproteinemia by RLP-Cholesterol Assay
- Headspace solid-phase micro-extraction and gas chromatography with micro-electron capture detection for the measurement of p,p'-DDE in rat whole blood and hair
- Haploid allele mapping of Y-chromosome minisatellite, MSY1 (DYF155S1), to a Japanese population
- Temporal changes in testis weight during the past 50 years in Japan
- Solid-phase microextraction and gas chromatography-mass spectrometry analysis of p, p'-DDE in biological samples
- Sudden Death of a Cocaine Abuser
- 韓国の機能性乳製品の現在と未来像
- An Enzyme-Linked Immunosorbent Assay (ELISA) for Measuring Human Erythrocytes Catalase
- Activation of Ceramidase and Ceramide Kinase by Vanadate via a Tyrosine Kinase–Mediated Pathway
- IS-029 Effect of intralesional or systemic dexamethasone for esophageal strictures in children(the 44th Annual Meeting of Japanese Society of Pediatric Surgeons)
- Irradiation inhibits vascular anastomotic stenosis in a canine model
- Aortic Root Replacement with a Stentless Bioprosthesis in a Patient with Giant Cell Arteritis
- Successful Surgical Treatment for Impending Rupture in Acute Type A Dissecting Aneurysm complicated With a Thoracoabdominal Aortic Aneurysm in an Octogenarian
- The protective effects of TV-12533, a novel sodium hydrogen inhibitor, and diazoxide on cardiac allgraffs from non-heart-beating donors
- Prognosis of patients with medically treated Stanford type B aortic dissection
- 1P306 1H1420 Decoding of temporal patterns of MAPKs by IEGs using ARX model(Mathematical biology,Oral Presentations,The 48th Annual Meeting of the Biophysical Society of Japan)
- Characterization of Subrepeat Regions within rDNA Intergenic Spacers of the Edible Basidiomycete Lentinula edodes(Biochemistry & Molecular Biology)
- Vacuum-assisted Closure System for the Treatment of Mediastinitis after Total Aortic Arch Replacement
- Hepatic Embolization through Extrahepatic Collateral Pathways after Hepatic Arterial Embolization for the Hepatocellular Carcinoma
- Chemical Kinetic Investigations of Ignition and Combustion Phenomena in a DI Diesel Engine Fueled with Methanol : Ignition Characteristics of Methanol Mixture
- Combustion and ignition characteristics in a glow assisted methanol DI engine (Optimization of slit geometries and glow-plug temperature)
- The Engorgement of the Great Veins and the Right Side of the Heart
- A STUDY ON ANGIOSPASM : A POSSIBLE MECHANISM FOR OCCLUSION OF THE AORTOCORONARY SAPHENOUS VEIN BYPASS GRAFTS : PROCEEDINGS OF THE 47th ANNUAL SCIENTIFIC MEETING OF THE JAPANESE CIRCULATION SOCIETY : Coronary Circulation
- Alteration in hippocampal and cerebral expression of glial fibrillary acidic protein following styrene exposure in rat
- Role of Chyromicron Remnant in the Progression of Coronary Atherosclerosis
- 海外レポート 現代中国市場における乳および乳製品の特徴(前篇)
- Screening procedure for the analysis of distigmine bromide in serum by high-performance liquid chromatography-electrospray ionization mass spectrometry
- Femtosecond Dynamics of Nonresonant Third-Order Optical Nonlinearity of 1-(3-thienyl)-3-(4-chlorophenyl)propene-1-one Crystal and Solution
- Remnant Lipoproteins from Patients with Pokkuri Disease (Sudden Death without Significant Coronary Stenosis) Enhances Coronary Vasospastic Activity through Rho-Kinase Upregulation
- IS-019 Prognostic factors for prenatally diagnosed congenital diaphragmatic hernia(International Session V,Better Life for Sick Children, Better Future for Pediatric Surgery,the 45th Annual Meeting of Japanese Society of Pediatric Surgeons)
- Successful Treatment for Rhabdomyosarcoma by Total Spondylectomy in a Child
- Identification of Five Phospho-β-glycosidases from Lactobacillus gasseri ATCC33323^T Cultured in Lactose Medium
- Langevin Equations in Quantized Field Theories
- Antiobesity Effects of Bifidobacterium breve Strain B-3 Supplementation in a Mouse Model with High-Fat Diet-Induced Obesity
- 細菌における細胞分裂メカニズムと乳酸菌の形態変化について
- Identification of a potent immunostimulatory oligodeoxynucleotide from Streptococcus thermophilus lacZ
- Effect of Transarterial Immunoembolization as Preoperative Treatment for Hepatocellular Carcinoma
- Determination of metaldehyde in human serum by headspace solid-phase microextraction and gas chromatography-mass spectrometry
- Simultaneous determination of dibucaine and naphazoline in human serum by monolithic silica spin column extraction and liquid chromatography-mass spectrometry
- Simultaneous determination of amitraz and its metabolite in human serum by monolithic silica spin column extraction and liquid chromatography-mass spectrometry
- Simultaneous Multi-Determination of Brain Trace Element Concentrations by Inductively Coupled Plasma Mass Spectrometry
- B-73. Diagnostic Value of the Anuerior Inferior Cerebellar Artery
- Surgical Strategy for Intracranial Endodermal Cyst : Two Case Reports
- Focal Leptomeningeal Metastasis Following Curative Surgery for Lung Cancer : Case Report
- Meson-Mass Generation by Instantons
- Successful treatment of severe refractory anastomotic stricture in an infant after esophageal atresia repair by endoscopic balloon dilation combined with systemic administration of dexamethasone
- Ramification and cleanliness
- Gene expression analysis for predicting gemcitabine resistance in human cholangiocarcinoma
- Mix-mode TiO-C_ Monolith Spin Column Extraction and GC-MS for the Simultaneous Assay of Organophosphorus Compounds and Glufosinate, and Glyphosate in Human Serum and Urine
- Oscillatory Motion of Natural Convection in Rectangular Cavity
- 海外レポート 現代中国市場における乳および乳製品の特徴(後篇)
- Activation of Ceramidase and Ceramide Kinase by Vanadate via a Tyrosine Kinase-Mediated Pathway
- 日本乳酸菌学会2010年度大会を終えて
- 見えない部分を大切に考える乳酸菌研究を次世代に
- ヒトABO式血液型を識別するプロバイオティック乳酸菌の発見とその将来的な利用戦略
- 海外レポート 第3回アジア乳酸菌シンポジウム(The 3rd ACLAB)に出席して
- パルミジャーノ・レッジャーノの乳酸菌研究で感じたこと
- Expression of a Biologically Active GFP-alpha(S1)-Casein Fusion Protein in Lactococcus lactis
- Spontaneous Hemorrhage From Orbital Cavernous Hemangioma Resulting in Sudden Onset of Ophthalmopathy in an Adult
- ウシをはじめとする家畜ミルクオリゴ糖研究の最近の進歩
- Hepatocellular Carcinoma that Relapsed 54 Months after Living Donor Liver Transplantation
- Class I/II hybrid inhibitory oligodeoxynucleotide exerts Th1 and Th2 double immunosuppression
- Spontaneous Hemorrhage From Orbital Cavernous Hemangioma Resulting in Sudden Onset of Ophthalmopathy in an Adult : Case Report
- 第3回アジア乳酸菌シンポジウム報告
- Phase I trial of preoperative intratumoral injection of immature dendritic cells and OK-432 for resectable pancreatic cancer patients
- Effects of Combustion Chamber Geometry in a Direct-Injection Diesel Engine : Comparison of Re-entrant and Conventional Chambers : Series B : Fluid Engineering, Heat Transfer, Combustion, Power, Thermophysical, Properties
- Pollen Morphology and Species-level Distinction of the Genus Fagus from the Hachiya Formation (Lower Miocene), Mizunami Group, Japan
- The Chemical Composition and the Energy Spectrum of Heavy Nuclei in the Cosmic Radiation above 10 GeV/nucleon
- Femtosecond Dynamics of Nonresonant Third-Order Optical Nonlinearity of 1-(3-thienyl)-3-(4-chlorophenyl)propene-1-one Crystal and Solution
- Multiple Intracranial Nodules Associated With Rheumatoid Arthritis: Case Report
- APPEARANCE OF RECTAL VARICES IN EXTRAHEPATIC PORTAL OBSTRUCTION AFTER TREATMENT FOR ESOPHAGO-GASTRIC VARICES : A CASE REPORT
- Development of the Status Map for Integration of Ramp Metering and Information Provision
- Determinant representation, Jacobi sum and de Rham discriminant(Algebraic Number Theory : Recent Developments and Their Backgrounds)