Synthesis and Characterization of High-T_c Superconducting Oxides by the Modified Citrate Gel Process
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概要
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High-T_c superconducting Y-Ba-Cu-O, Bi-Ca-Sr-Cu-O, and Tl-Ca-Ba-Cu-O materials were synthesized using a modified citrate precursor process. Ethylenediamine was used to neutralize the metal citrate solution and facilitate the complex formation. Highly homogeneous and viscous gel without any precipitation was obtained. In the Tl-Ca-Ba-Cu-O system, the Ca-Ba-Cu-O precursor was first prepared by the sol-gel method, then mixed with thallium oxide for final sintering. The complex formation was monitored by UV/VIS spectrophotometry. The thermal decomposition of gels and the formation of superconducting phases had been studied using IR, DTA, TGA, and XRD. This process is highly reproducible and leads to powders with excellent homogeneity and small particle size for easy sinterability.
- 社団法人応用物理学会の論文
- 1989-12-20
著者
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Wu P
Materials Research Laboratories Industrial Technology Research Institute
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Liu R
Irc In Superconductivity:materials Research Laboratories Industrial Technology Research Institute:de
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Liu R.
Department Of Chemistry National Taiwan University
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Chang C.
Department Of Anatomy Taipei Medical University
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Wang W
Inst. Taiwan Hsinchu Twn
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Wu P.
Materials Research Laboratories Industrial Technology Research Institute
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Wu P.
Materials Research Laboratories Industrial Technology Resarch Institute
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Chang C
Department Of Chemistry National Tsing-hua University Hsinchu And Institute Of Atomic And Molecular
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LIU R.
Materials Research Laboratories, Industrial Technology Research Institute
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WANG W.
Chung Shan Institute of Science and Technology
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