The Synthesis and Nuclear Magnetic Resonance Spectra of Epimeric 16-Deuterio-13α-androstan-17-ols

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概要

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• Four epimeric 16-deuterio-5α, 13α-androstane-3β, 17-diols were prepared starting from 3β-hydroxy-5α, 13α-androstan-17-one, and the conformation of ring D in 13α-steroids is discussed based upon the correlation of dihedral angles with the observed coupling constants of H16,17. The chemistry of the 16β, 17β-epoxy and Δ^<16> compounds is also described.

• 公益社団法人日本薬学会の論文
• 1968-09-25

著者

• Fishman Jack

  Institute For Steroid Research Montefiore Hospital

• 碓氷 昌宏

  Pharmaceutical Institute, Tohoku University

• 碓氷 昌宏

  Pharmaceutical Institute Tohoku University

関連論文

• The Bromination of 13α-Androstan-15-one
• The Synthesis and Nuclear Magnetic Resonance Spectra of Epimeric 16-Deuterio-13α-androstan-17-ols
• The Synthesis and Conformational Analysis of Epimeric 17-Bromo-14β-androstan-16-ones
• A Nuclear Magnetic Resonance Spectral Study of 5α, 13α-Androstanes
• The Synthesis and Nuclear Magnetic Resonance Spectra of Epimeric 16-Deuterio-14β-androstan-17-ols
• Rearrangements of the 16,17-Ketols of 13α-Androstanes
• The Synthesis and Conformational Analysis of α-Bromo-16-ketones of 13α-Androstanes

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