Studies on Cinnolines. III. Oxidation of 5-and 8-Nitrocinnoline
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概要
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The oxidation of 5-nitrocinnoline (I) with hydrogen peroxide in acetic acid, and with persulfuric acid in sulfuric acid afforded 5-nitrocinnoline 1-oxide (II), 5-nitrocinnoline 2-oxide (III), and 4-nitroindazole (IV). The Oxidation of 8-nitrocinnoline (V) with hydrogen peroxide in acetic acid, with hydrogen peroxide, with phthalic monoperacid, with hydrogen peroxide in 10% sulfuric acid, and with persulfuric acid in sulfuric acid afforded 8-nitrocinnoline 2-oxide (VI), 7-nitroindazole (VII), and 8-nitro-4-cinnolinol (VIII). On the other hand, the oxidation of V with chromic acid in acetic acid gave only VIII with recovery of V.
- 公益社団法人日本薬学会の論文
- 1965-06-25
著者
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鈴木 郁生
国立衛生試験所
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鈴木 郁生
National Hygienic Laboratory
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中島 利章
Central Research Laboratories, SS Pharmaceutical Co., Ltd.,
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中島 利章
National Institute of Hygienic Sciences
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長沢 奈都子
National Institute of Hygienic Sciences
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中島 利章
Central Research Laboratory Ss Pharmaceutical Co. Ltd.
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